Studying the effect of particle size on the antibacterial activity of some N-nicotinyl phosphoric triamides

Using ultrasonic top-to-down method, nanoparticles of two N-nicotinyl phosphoric triamides: C₅H₄NC(O)NHP(O)R, R?=?4-CH₃-NC₅H₁₀ (1), (CH₃)₃CNH₂ (2) were prepared for the first time and characterized by ³¹P, ¹³C, ¹H NMR, FTIR, scanning electron microscopy, energy dispersive X-ray. The average particle size of 1 and 2 were 60–70 and 40–50?nm, respectively, and the morphology was spherical for 1 and rod for 2. Solid state (powder) antibacterial effect of these compounds and two other similar reported ones, in their macro- and nanosizes, were evaluated with colony counting method on one Gram-positive (Staphylococcus aureus) and one Gram-negative (Escherichia coli) bacteria in Brain–Heart infusion culture medium. Results showed that all the macro- and nanosized compounds, except macrosized 1, were antibacterial and all nanoscaled ones had stronger antibacterial activity than their macroscaled analogues. The most effect of the particle size was observed for 1: by decreasing the particle sizes, the antibacterial activity state of 1 was changed from inactive (for macro) to potent (for nano).     

载气热提取法测定熔敷金属中扩散氢收集条件的探究

探究了GB/T 3965—2012《熔敷金属中扩散氢测定方法》中载气热提取法收集条件对测定扩散氢含量的影响,并与水银法进行了对比。研究结果表明,样本炉温设定为400℃,A型试块的内部温度大约在51 min时稳定在358℃左右,B型试块内部温度大约在27 min时稳定在391℃左右;载气热提取法电信号曲线收集结束点的电信号及斜率均接近0时获得的结果与水银法具有较好的一致性。     

Multiphase topology optimization with a single variable using the phase-field design method

In this study, a multimaterial topology optimization method using a single variable is proposed by combining the solid isotropic material with penalization method and the reaction-diffusion equation. Unlike ordinary multimaterial optimization, which requires several variables depending on the number of material types, this method intends to represent various materials as one variable. The proposed method combines two special functions in the sensitivity analysis of the objective function to converge the design variable into prespecified density values defined for each of the multimaterials. The composition constraint based on a normal distribution function is also introduced to estimate the distribution of each target density value in a single variable. It enables density exchange between multiple materials by increasing or decreasing the amount of a specific material. The proposed method is applied to structural and electromagnetic problems to verify its effectiveness, and its usefulness is also confirmed from the viewpoint of cost and computation time.     

Biologically Inspired Design of Context-Aware Smart Products

The rapid development of information and communication technologies (ICTs) and cyber–physical systems (CPSs) has paved the way for the increasing popularity of smart products. Context-awareness is an important facet of product smartness. Unlike artifacts, various bio-systems are naturally characterized by their extraordinary context-awareness. Biologically inspired design (BID) is one of the most commonly employed design strategies. However, few studies have examined the BID of context-aware smart products to date. This paper presents a structured design framework to support the BID of context-aware smart products. The meaning of context-awareness is defined from the perspective of product design. The framework is developed based on the theoretical foundations of the situated function–behavior–structure ontology. A structured design process is prescribed to leverage various biological inspirations in order to support different conceptual design activities, such as problem formulation, structure reformulation, behavior reformulation, and function reformulation. Some existing design methods and emerging design tools are incorporated into the framework. A case study is presented to showcase how this framework can be followed to redesign a robot vacuum cleaner and make it more context-aware.     

复合管膜的润湿性及过滤污水机理

为了研究多孔复合管膜对钢铁产业污水的过滤性能及其过滤机理，采用静滴法做了水滴和油滴在复合管膜上的润湿性研究。采用扫描电镜、EDS等手段分析了使用前后的多孔复合管膜外壁及内壁的结构及成分，分析了含油污水中固体颗粒及油的过滤机理，并利用视频光学接触角测量仪测量水滴和油滴在复合管膜上接触角随时间的变化速率。结果表明，在污水过滤过程中，水中小于管膜表层微孔孔径的氧化铁等杂质进入复合管膜内部，无法随水流穿过复合管膜膜层，积累在管膜内部；随着管膜使用时间延长，氧化铁等杂质在复合管膜内部积累量增多。水在复合管膜上的润湿性良好，油滴在复合管膜上是不润湿的。     

上海市火力发电行业能源计量现状分析

能源计量与节能监测、能源审计、能源统计、能源利用状况分析是用能单位能源管理和节能工作的基础。通过对本市部分火力发电企业的现场调研，针对性地提出改进建议，以期帮助用能单位增强能源计量在节能减排工作中的有效性。     

A CCD-ADI method for two-dimensional linear and nonlinear hyperbolic telegraph equations with variable coefficients

In this paper, a combined compact finite difference method (CCD) together with alternating direction implicit (ADI) scheme is developed for two-dimensional linear and nonlinear hyperbolic telegraph equations with variable coefficients. The proposed CCD-ADI method is second-order accurate in time variable and sixth-order accurate in space variable. For the linear hyperbolic equation, the CCD-ADI method is shown to be unconditionally stable by using the Von Neumann stability analysis. Numerical results for both linear and nonlinear hyperbolic equations are presented to illustrate the high accuracy of the proposed method.     

Extended dissipativity-based non-fragile control for multi-area power systems with actuator fault

This paper addresses the issue of reliable load frequency control design of an uncertain multi-area power system with constant time delays and disturbances via non-fragile sampled-data control approach. In particular, the parameter uncertainties are assumed to be randomly occurring which are described by the Bernoulli distributed sequences. By constructing a suitable Lyapunov–Krasovskii functional together with Wirtinger-based inequality, a new set of sufficient conditions in terms of linear matrix inequalities is obtained to ensure the asymptotic stability and extended dissipativity of the multi-area power system not only when all actuators are operational, but also in case of some actuator failures. Finally, simulation results are conducted to validate the effectiveness of the proposed control design technique.